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pinus_sylvestris_l [2018/06/29 14:23]
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pinus_sylvestris_l [2020/02/07 11:38] (aktuell)
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| [Tümen, İbrahim, and Markku Reunanen. "A comparative study on turpentine oils of oleoresins of Pinus sylvestris L. from three districts of Denizli." Records of Natural Products 4.4 (2010): 224-229] [[http://acgpubs.org/RNP/2010/Volume%204/Issue%201/27-RNP-1008-297.pdf]] | [Tümen, İbrahim, and Markku Reunanen. "A comparative study on turpentine oils of oleoresins of Pinus sylvestris L. from three districts of Denizli." Records of Natural Products 4.4 (2010): 224-229] [[http://acgpubs.org/RNP/2010/Volume%204/Issue%201/27-RNP-1008-297.pdf]] |
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| "...the current study aimed to elucidate the smell of pine wood by analysing the odour-active substances in three Pinus sylvestris L. samples... dedicated odorant analysis techniques such as gas chromatography-olfactometry (GC-O) and aroma extract dilution analysis (AEDA) were applied and successfully detected 44 odour-active compounds; of these, 39 substances were successfully identified by gas chromatography-mass spectrometry/olfactometry (GC-MS/O) and two-dimensional gas chromatography-mass spectrometry/olfactometry | To elucidate the smell of pine wood, solvent-assisted flavour evaporation (SAFE) of volatiles from pine wood shavings followed by dedicated odorant analysis techniques such as gas chromatography-olfactometry (GC-O) and aroma extract dilution analysis (AEDA) was applied. Of 44 odour-active compounds, 39 were identified by two-dimensional gas chromatography-mass spectrometry/olfactometry (2D-GC-MS/O). The majority of the identified odorants were fatty acid degradation products, plus some terpenoic substances and odorous substances resulting from the degradation of lignin. Highest flavour dilution factors (FD>=243) showed α-pinene (woody resinous), hexanal (green grassy), octanal (citrus), (E)-non-2-enal (fatty), linalool (citrus), (E)-dec-2-enal (fatty), (E,E)-nona-2,4-dienal (fatty), pentanoic acid (cheesy), (E,E)-deca-2,4-dienal (fatty), heptanoic acid (pepperoni-like, plastic), δ-octalactone (coconut), γ-nonalactone (peach), (E,Z,Z)-trideca-2,4,7-trienal (fruity blood-like metallic), δ-nonalactone (sweet coconut), nonanoic acid (leather artificial soapy), sotolone (savoury), α-bisabolol (balsamic pepper-like), phenylacetic acid (honey-like), vanillin (vanilla-like), 3-phenylpropanoic acid (vomit-like fruity), an unidentified androstenone-like substance (perfume-like) and thymoquinone (pencil-like). \\ |
| (2D-GC-MS/O). Among the main odorants found were (E,E)-nona-2,4-dienal, vanillin, phenylacetic acid, 3-phenylpropanoic acid, δ-octalactone and α-pinene, all of them having been detected with high flavour dilution factors during GC-O analyses. The majority of the identified odorants were fatty acid degradation products, plus some terpenoic substances and odorous substances resulting from the degradation of lignin. Although some of the detected substances have previously been reported as constituents of wood, 11 substances are reported here for the first time as odour-active compounds in wood, amongst them heptanoic acid, γ-octalactone, δ-nonalactone and (E,Z,Z)-trideca-2,4,7-trienal." \\ | [Schreiner, L., Bauer, P., & Buettner, A. (2018). Resolving the smell of wood-identification of odour-active compounds in Scots pine (Pinus sylvestris L.). Scientific reports, 8(1), 8294] |
| [Schreiner, L., Bauer, P., & Buettner, A. (2018). Resolving the smell of wood-identification of odour-active compounds in Scots pine (Pinus sylvestris L.). Scientific reports, 8(1), 8294] \\ | |
| [[https://www.nature.com/articles/s41598-018-26626-8]] | [[https://www.nature.com/articles/s41598-018-26626-8]] |
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| | Using stable isotope dilution analysis (SIDA) and odor activity values (OAVs) calculated on the basis of odor thresholds determined in cellulose, hexanal, octanal, (E)-non-2-enal, p-cresol, vanillin, and thymoquinone were the dominant odorants for wood odor of several softwood species (Pinus sylvestris, Larix decidua, Calocedrus decurrens, Abies concolor, and Picea abies). OAVs ≥ 1 were obtained for p-cresol (2), hexanal (OAV=6), octanal (374), (E)-non-2-enal (163), and vanillin (10). \\ |
| | Of all wood samples, the highest concentration of α-pinene was observed in Scots pine wood (122 mg/kg), but with an OAV<1. \\ |
| | "Even though α-pinene did not exceed an OAV > 1 in the wood samples, this compound was added to the recombinate for several reasons: On the one hand, during sensory evaluation, the attribute resin-like was rated with the highest values for the pine wood. Thus, the resin-like–smelling α-pinene might have an impact on the odor, since it was observed as the only odorant representing that odor impression. Furthermore, α-pinene was recorded with high-flavor dilution (FD) factors. In concordance with that, we found that preparation of the recombinates in the absence of α-pinene resulted in a lack of the resin-like odor. One reason for not exceeding an OAV ≥ 1 might be a potential synergism with other wood constituents, leading to an increased resin-like odor impression." \\ |
| | [Schreiner, Linda, Eva Ortner, and Andrea Buettner. „Nosy confirmation: reconstitution of the characteristic odor of softwood via quantitative analysis and human sensory evaluation.“ Analytical and Bioanalytical Chemistry (2019): 1-13] |
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